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Seperating liquids from a mixture in previous experiments has shown me that bubbles in your final stew is bad. Yes purging is a good try, you probably mean the iso, and a few drops of h2o then oil bath, or over heat in a vacuum.
This still tastes like butane on the second hit. And yes it could be a wax(plant contam)as some strains react different to the purging process leaving a butter waxy looking product rather than a clear goo.
The chromatography seperation I hear is the way to go to test clean, in analysis.
-------------------- All of the statements and posts I make or have made are fake. I just found all the pictures and copied and pasted them here. I am in no way associated with any of the materials discussed here. I'm just bored, and lame.
Quote: Dephect said: BHO is the shit. A easy way to get it to a easy handled texture is just to let it sit. After you evap put a heating pad underneath it on high to purge. Go to bed or do something. The longer you cook it like that the more it hardens and its good because it ensures all the butane is gone.
BHO is better then Bubble in my eyes.. I like using solvents more to make my stuff.. All though I wouldn't mind getting a bubble bag + washer unit so I can make a large amount of bubble with out the work that goes into it.
Oh yeah and I use Vector Quintuple Purified Butane. Its good stuff.
I hope thats not your idea of purging.
-------------------- All of the statements and posts I make or have made are fake. I just found all the pictures and copied and pasted them here. I am in no way associated with any of the materials discussed here. I'm just bored, and lame.
Quote: Look at those bubble in your final product. Learn to filter it better.
You really didn't even bother to read my post did you?
Quote: I obviously didn't purge the butane well enough because a.) I was a little impatient, b.) it's such a tiny amount and c.) I'm just testing things out for the moment and don't really care too much about removing all impurities.
Quote: Next time I will have a nice hot oil bath that my extraction plate will sit in and I'll possible re-dissolved in some ethanol for a final purge.
Quote: You really need a Chromatography Column, but you can do it by other mean
Oh yah, let me reach into my back pocket and pull out my 10-20 K and the Chemistry degree that I don't have.
Seriously bud, you need to come down off your high horse here (no pun intended) and start contributing more to this forum other than shit talking with nothing to back it up. I see you post a lot about we're all doing it wrong and your methods are so much better, but yet, I see no teks, no pictures, nothing from you in this area that would help others and possibly not make yourself look like a complete douche bag.
Sorry, I am passionate about pure hash oil. Very pure, and you noticed the problems i did in my quest to make good hash oil. I was excited and sounded, was, a bit over bearing.
If we all try different things, and are pushed by our peers in a common direction we can have the recipe for the best oil ever.
Some of the best i've made were extracting everthing with Iso, then adding Et20 and some distilled h2o to create the seperation. Remove the top layer, and evap, or you can isomerized with hydrochloric acid.
Or if you like butane so much. Kief all your material, to shit, and decarb in the oven. Exhaust a can or two of butane into a mason, and add all the kief(or hash) Filter with your preferred micron size, or coffee filter. Evaporate Solvent * And clean with your preffered method
way bigger yield, less possibility of plant material, and no pressurized bomb in your hand, just watch for sparks.
Or you can take water hash, all microns,and re liquify with Iso, Filter in 25 mic or less, and evap. Looks like Heroin, melts like butane, just h2o and Iso only.
food for thought
-------------------- All of the statements and posts I make or have made are fake. I just found all the pictures and copied and pasted them here. I am in no way associated with any of the materials discussed here. I'm just bored, and lame.
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