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Also just so everyone learns from my mistakes. One big jar of solvent in the freezer can take a couple weeks to get a decent amount of crystals on the bottom where when I used 2 smaller jars it only took 12 hours.
Yeah man the more solvent the longer it'll take to precipitate. I usually evaporate the solvent down to only a few milliliters and the crystals drop out pretty quickly. If you feel like it next time try evaping the contents of one of your little jars down to about half or even a third of what you've got in there and it should take even less time to fully precipitate.
I have found that an ice bath precip also works well, or using the tall POM tea jars in the freezer. The larger surface area relative to volume allows for much faster cooling and IMO a better precip.
Also remember the whips when blazing deem.
And good work you got there, my own mother would be proud.
-------------------- [quote]hemostats said: like i said before
quite simply, you are a nuisance while i am a smooth criminal.[/quote]