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InvisibleDeadkndys420
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Registered: 08/28/12
Posts: 8,702
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Clean and Easy STB * 5
    #718683 - 03/01/14 01:26 PM (10 years, 7 months ago)

Well this is not really a "other growable" but I thought this was the most relevant place to post this.


Below is a nice writeup on extracting DMT.
Enjoy.

*it is recommend to replace plastic items with glass.
Quote:



1. 445.9g MHRB was broken up and finely shredded in a glass blender

2. 15 tbsp NaOH was added to 3,400 mL dH2O (Always add lye to water).

3. MHRB was combined with basic H2O in a 1 gal HDPE water jug.
(If the mixture is basic enough, it will turn a slippery black color)

4. This mixture was allowed to sit for 1 hr. During the last 30 min, the
jug was placed in a hot water bath. The jug was shaken periodically
throughout the whole hour.

5. 250 ml vm&p naphtha was added to the jug. The jug was shaken
for ~15 min



6. After 15 min the naphtha was separated off with this handy syringe
contraption (hell of a lot easier than a turkey baster). It was made
by gluing two meat injector syringes together, and then gluing some
1/4" Polyethylene tubing to the tip.

If you happen to suck up some basic sludge, don't worry, just empty
the syringe into a pyrex measuring cup. The solvent can then easily
be poured off of the tiny bit of sludge you may have sucked up


*Apparently, using two syringes is necessary so that the naphtha does
not come in contact with the rubber on the plunger. because
naphtha will melt/corrode the rubber on shitty meat injector syringes.




I suspect if one had access to lab grade materials that don't degrade
with chemical contact, this could be avoided.


7. 4 naphtha pulls of 200-250ml were done in total. Before the 3rd pull,
another 100ml of basic dH2O was added to the mixture

8. Separated naphtha was placed into pyrex baking dishes. Lights were
used as a heat source to accelerate the evaporation of 2/3 of the
solvent.

*If you decide to do this, it is very important to pay attention to
your evaporation trays, checking them constantly*



9. The remaining 1/3 of solvent in each pan was left to evaporate for 24
hrs. Screens were made out of some wood and some nylon
stockings. They were very cheap to make, and are highly
recommended if one will be going the evaporation route.




*Optimism skyrocketed when the first pull began to crystallize while the
naphtha was still warm*

10. The next day the screens were removed to find many beautiful
crystals.

First Pull (still drying):



Dried:


Second Pull:


Third Pull:




Fourth Pull:



The 1st pull yielded 1.9g of large, tannish crystals, mixed in with whiter powdery crystals:



2nd pull yielded 1.1g of white powdery crystals:



3rd pull yielded 1.2g of white powdery crystals:


4th pull yielded 0.6g of white powdery crystals:




Total Yield: 4.8g very clean spice, with no defats, and no washes.

(1st Pull on the left, 2nd, 3rd & 4th pulls combined on right)



Edited by Deadkndys420 (01/18/15 08:01 PM)

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Invisiblenannybooboo
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Registered: 04/23/11
Posts: 3,089
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #718941 - 03/02/14 03:06 PM (10 years, 7 months ago)

Ohhh yeaaaaahh!

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InvisibleP-O


Registered: 10/08/11
Posts: 17,891
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #718994 - 03/02/14 05:00 PM (10 years, 7 months ago)

fuck ya :hi5:

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InvisibleCrushNazT
Male


Registered: 07/23/13
Posts: 927
Loc: Colorado Flag
Re: Clean and Easy STB [Re: P-O] * 1
    #718995 - 03/02/14 05:04 PM (10 years, 7 months ago)

is it even possible to get MHRB anymore? i havent seen it for a couple years.

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InvisibleDeadkndys420
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Registered: 08/28/12
Posts: 8,702
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Re: Clean and Easy STB [Re: CrushNazT] * 1
    #719003 - 03/02/14 05:16 PM (10 years, 7 months ago)

I saw a vendor selling powdered MHRB for 140 a kilo

I plan on buying some on Friday.

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InvisibleCrushNazT
Male


Registered: 07/23/13
Posts: 927
Loc: Colorado Flag
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #719031 - 03/02/14 08:18 PM (10 years, 7 months ago)

Quote:

Deadkndys420 said:
I saw a vendor selling powdered MHRB for 140 a kilo

I plan on buying some on Friday.




let me know how that goes. i'd like to pick one up if i could.

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InvisibleDeadkndys420
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Posts: 8,702
Loc: █████
Re: Clean and Easy STB [Re: CrushNazT] * 1
    #719415 - 03/05/14 07:01 PM (10 years, 6 months ago)

Turns out that vendor was no good. (broken site):thumbdown:

I also found out that looking for MHRB under  Mimosa Hostilis,Jurema bark, etc is near impossible. But as it turns it people are selling it under " Acacia Tenuiflora Tepezcohuite" instead of MHRB. Someone on Ebay is selling a kilo for 110.
:crazy2:

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InvisibleP-O


Registered: 10/08/11
Posts: 17,891
Re: Clean and Easy STB [Re: Deadkndys420] * 2
    #719418 - 03/05/14 07:22 PM (10 years, 6 months ago)

I emailed my old vendor about MHRB and cactus chips, and this is the reply i got:


Quote:

Thanks for your message.

Unfortunately, we don't know when or even if we'll supply the Mimosa as the governments and customs don't allow importation and exportation of this wonderful incense anymore. We find this situation very sad, since this plant was great to make nice incense and to treat skin problems.

For the Peruvian Torch we are presently back order but we should receive some more within the spring. do you want to be notice when it get back on stock?

Also , we supply the Acacia Confusa Root bark which is a very similar incense to the Mimosa. Here are the prices for the availables quantities:





so ya apparently acacia is the new thing people are using .

"We find this situation very sad, since this plant was great to make nice incense and to treat skin problems"


:lol:

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InvisibleDeadkndys420
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Posts: 8,702
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Re: Clean and Easy STB [Re: P-O] * 1
    #719635 - 03/06/14 09:21 PM (10 years, 6 months ago)

Anyone have any idea on what the screens are for?

It looks like they are on top of the trays to prevent dust etc. :shrug:

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Invisiblenannybooboo
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Registered: 04/23/11
Posts: 3,089
Re: Clean and Easy STB [Re: Deadkndys420] * 4
    #719751 - 03/07/14 06:16 PM (10 years, 6 months ago)

Ya probably to prevent dust and other unwanted things like wombats and pigeon feathers, but still have sufficient airflow at the top.

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InvisibleDr. SiekadellykM
Question Everything!
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Folding@home Statistics
Registered: 04/20/09
Posts: 9,365
Loc: Ketamine Flag
Re: Clean and Easy STB [Re: nannybooboo] * 3
    #719754 - 03/07/14 06:53 PM (10 years, 6 months ago)

Yeah I always get pigeon feathers in my product if I don't cover it with screen while evap.


--------------------
The Kratom Report...

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InvisibleDeadkndys420
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Posts: 8,702
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Re: Clean and Easy STB [Re: Dr. Siekadellyk] * 2
    #719755 - 03/07/14 07:10 PM (10 years, 6 months ago)

Quote:

Dr. Siekadellyk said:
Yeah I always get pigeon feathers in my product if I don't cover it with screen while evap.



:lol:

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Invisiblethedrake
N00B
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Registered: 10/04/11
Posts: 101
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #720245 - 03/09/14 07:53 PM (10 years, 6 months ago)

havent had dmt in a while. this thread is making me want some :tripping:


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InvisibleDeadkndys420
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Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #739275 - 07/08/14 09:00 AM (10 years, 2 months ago)

Bump.

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InvisibleP-O


Registered: 10/08/11
Posts: 17,891
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #739339 - 07/08/14 04:04 PM (10 years, 2 months ago)

broke through yet?

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InvisibleDeadkndys420
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Posts: 8,702
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Re: Clean and Easy STB [Re: P-O] * 1
    #739347 - 07/08/14 04:48 PM (10 years, 2 months ago)

Nah not yet. I can't seem to hold it in long enough. Gonna try making a meth bong and hope that helps next time.

Even after using heptane to refine it some more it is still harsh as fuck.

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InvisibleDeadkndys420
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Registered: 08/28/12
Posts: 8,702
Loc: █████
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #739348 - 07/08/14 04:52 PM (10 years, 2 months ago)

Also if someone is going the syringe route I highly recommend buying a glass one. Plastic will corrode too easily and is a PITA to deal with no matter what adhesive/silicone you use.


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Offlinennn-yan
Shaman Norse Warrior


Registered: 02/03/13
Posts: 103
Last seen: 5 years, 10 months
Re: Clean and Easy STB [Re: Deadkndys420] * 2
    #739569 - 07/10/14 06:24 PM (10 years, 2 months ago)

Sorry for the bump but i feel like this should be addressed.

Using plastic can still be dangerous, Use glass so no unwanted Phthalates are present

Please read more for you safety and knowledge!
No casualties please. :scat:
https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=26324

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OfflineSmokeSomeHash
Littlest pee pee on da block
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Registered: 02/26/13
Posts: 1,555
Loc: murica Flag
Last seen: 8 years, 7 months
Re: Clean and Easy STB [Re: Deadkndys420] * 1
    #745433 - 08/27/14 09:18 PM (10 years, 1 month ago)

First off, super sick post.

Second...ive never tried it but ive heard that you can dab DMT off a nail and dome set up

i dunno how that would compare to a meth bong?


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InvisibleDeadkndys420
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Registered: 08/28/12
Posts: 8,702
Loc: █████
Re: Clean and Easy STB [Re: SmokeSomeHash] * 1
    #745499 - 08/28/14 03:58 PM (10 years, 1 month ago)

As long as the temps are right I don't see why it wouldn't work.

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